Food is of paramount importance to the people, and feed is of paramount importance to animal husbandry. Whether ordinary people can eat reliable meat and drink reliable milk depends on feed. In recent years, incidents of adding "growth hormone" and "protein essence" to animal feed have occurred frequently, seriously endangering the quality of animal food. Therefore, the issue of feed has become a hot topic of concern for the general public and has attracted the attention of relevant national departments. To ensure the quality of feed and feed additives, the National Regulations on the Administration of Feed and Feed Additives2012year5the moon1Formally implemented from [date].2012year10the moon9The Ministry of Agriculture of Japan has also reviewed and approved the "License Conditions for Feed Enterprises" and "License Conditions for Mixed Feed Additive Enterprises" in accordance with the regulations2012year12the moon1Implemented from [date].
The Regulation clearly stipulates that feed and feed additive enterprises have "necessary product quality inspection institutions, personnel, facilities, and quality management systems"; The "License Conditions" have put forward more clear requirements for product quality inspection. Enterprises * * have a feed testing laboratory and are equipped with effective liquid chromatography (equipped with ultraviolet detectors) or atomic absorption spectrophotometry (equipped with flame atomic spectrometers and element lamps for the tested items) or both according to their own feed types.
Our company has developed a comprehensive feed testing laboratory solution in accordance with national policies, which includes pre-sales consultation, equipment matching, testing method training, after-sales service, and * * standardized servicesThe results are accurate and reliable, with good detection limits, widely applicable for the determination of various vitamins in compound feed, concentrated feed, compound premix feed, and vitamin premix feed.It is one of the standard instruments for ensuring feed quality by successfully passing the certification system acceptance.
1、 Characteristics of effective liquid chromatography for vitamin detection in feed:
1The entire system adopts a modular structure design, with components such as infusion pumps and detectors freely matched, and strong scalability; All key components are imported with original packaging, making analysis more reliable and performance more stable.2The high-pressure infusion pump has a high pressure resistance of up to42MpaBy using electronic compensation, the flow pressure is more stable and the reproducibility is better.3The ultraviolet detector adopts a straight band optical method, with a simple structure, easy maintenance, fast self checking speed, high wavelength accuracy, and good reproducibility.
2、 Main technical parameters: 1Infusion method: Double plunger series pump2Flow rate range:0.001-9.999ml/min 3Work pressure:42Mpa 4Scope of testing:(190-700)mm,Single wavelength5Control: Panel control or workstation reverse control.
3、 Effective liquid chromatography for detecting vitamins in feedLC-3000Ito configure:
1、P3000High pressure infusion pump1Unit (single pump)2、UV3000UV detector1Taiwan3、7725iManual injection valve1A (American)4、4.6mmx150mm x5um C18chromatographic column1Root5Chromatographic Column Temperature Chamber1Taiwan6、CXTH-3000Chromatography workstation7Startup toolkit1Set up8、1 analytical dynamic mixer (Germany) 9, 1 solvent tray 10, 1 solvent filter, 1 vacuum pump, and 1 ultrasonic (purchased separately, required for first-time use).
4、 Working principle:
Fat soluble vitamins: alkaline solution saponification sample, solvent extraction, effective liquid chromatography reverse phase or forward analysis
Water soluble vitamins: extracted from aqueous solution and analyzed by reverse liquid chromatography.
5、 Laboratory analytical instruments and equipment:
1. LC3000 effective liquid chromatography instrument
2. Liquid chromatography column: C18150mm × 4.6mm × 5 μ m;
3. One ten thousandth analytical balance
4. Round bottom flask (with reflux condenser)
5.Nitrogen blower orthermostat water bath
6.High speed centrifuge+
7.Ultrasonic cleaning machine, solvent filter, and vacuum pump
8.Solid phase extraction device
9. Reagents and standards
VIExperimental conditions:
Mobile phase: methanol+water=95+5; Flow rate: 1.0mL/min;
Temperature: room temperature; Injection volume: 20 μ L;
Wavelength: 326nm for vitamin A, 264nm for vitamin D3, and 280nm for vitamin E
seven、answerScope of application:
Detecting various vitamins in feed, such as:vitaminA vitaminD3 vitaminE、VitaminK3vitaminB1vitaminB2vitaminB6vitaminB12Niacin, folate, pantothenic acidd-biotinDetection, etc,At the same time, it shouldinstrumentstillCan be expandedconfigurationDetecting residues of various drugs.
8、 Case: VitaminsAStandard effective liquid chromatography chart
Related links: 1、 Effective liquid chromatography analysis scheme for amino acid detection in feed
2、 Effective liquid chromatography method for detecting the content of quinoxaline in feed
3、 Determination of Organic Acid Content in Feed Additives by Effective Liquid Chromatography
4、 Effective liquid phase analysis scheme for detecting Sudan Red dye in feed
5、 Liquid chromatography detection scheme for melamine in feed
6、 Detection scheme of nutrient elements and heavy metals in feed using atomic absorption spectrophotometer
7、 Effective liquid chromatography detection scheme for oxytetracycline in feed
8、 Effective liquid chromatography detection scheme for dopamine hydrochloride in feed
9、 Determination of clenbuterol hydrochloride in feed by liquid chromatography detection scheme
10、 Determination of Calcium, Copper, Iron, Magnesium, Manganese, Potassium, Sodium, and Zinc Content in Animal Feed by Atomic Absorption Spectroscopy
11、 Determination of Cobalt in Feed by Atomic Absorption Spectroscopy
12、 Determination of lead in feed by atomic absorption spectrometry
13、 Determination of cadmium in feed by atomic absorption spectrometry
14、 Determination of Chromium in Feed by Atomic Absorption Spectroscopy
companyThe clothingaffairAdvantages:
1The companyofafter-sale serviceEngineers have undergone chemical analysis、Training on instrument repair and maintenance,They can maintain and repair various components,To ensure that your instrument runs smoothly and quickly,Can guarantee to solve your problems quickly.
2、Timely telephone technical support----faultarrangeExcept for experts answering your calls,Provide timely solutions to problems.
3、****Service----distributionProvide high-quality services within the scope of * * * *.
4、flexiblefastResponse time after phone repair report, providetimelyGuidance orDoor to door problem-solving.
524 hours non-stopOnline Instrument Problem Answering.
6、There are free and irregular chromatography training courses every year.The content includes chromatographic principles、analysis、application、Technical instrument operation,helpAssist the causeObstacle removal and maintenance.
