1、 Instrument Introduction:
Complete configuration
STA 449 F5 Jupiter ®Specially designed for a vacuum sealed structure according to your needs. The instrument configuration is complete, and the software and hardware functions are fully designed, suitable for various application fields such as ceramics, metals, inorganic materials, and construction.
Excellent synchronous thermal analysis performance
The balance system can provide a sufficiently large sample size and measurement range (the largest)35g)At the same time, it has high resolution(0.1 μg)And low drift (inμgWithin the range, combined with high sensitivityDSCPerformance can be tested on various samples over a wide temperature range.
Unique combination-accurateTGA-DSCAnd large capacityTGA
At room temperature to 1600℃ Within a wide temperature range,STA449F5 ®Can achieve high precision and high repeatabilityTGAandDSCMeasurement.TGASupport large-scale sample testing, with the largest crucible volume capable of reaching5 cm3.
Top mounted sample-Mature thermal balance design scheme
STA 449 F5 Jupiter ®The top loading structure is adopted, which has long been the standard method for balance measurement in the laboratory. The reason is simple, this design combines the characteristics of superior performance and simple operation.
2、 Technical parameters (continuously updated)
●Temperature range:RT...1600℃(Sample temperature)
●Furnace body:SiCFurnace body, motor-driven automatic lifting, easy and safe operation
●Heating rate:0.001 ... 50K/min
●Sensor:
- TGA-DSC(Standard configuration)
- TGA-DSCASC(Optional, suitable for configurations with automatic sampler)
- TGA(Optional, for large sample sizes)
- TGA-DTA(Optional)
●Users can quickly and conveniently replace different sensors themselves
●Vacuum tightness:10-2 mbar
●AutoVacIntegrated software controlled automatic vacuum system
●Atmosphere: Inert, Oxidative, Static, Dynamic
●Automatic sampler(ASC):20 Position of crucible (configuration)II)
●Gas flow control: integrated 3 Road mass flow meter(1 Road protection gas,2 Road blowing air
●Temperature resolution:0.001 K
●Balance resolution:0.1 μg(Full range)
●BeFlat ®Built in, automatically adjusts buoyancy effects related to crucible type, atmosphere, heating rate, and other factors to obtain a smooth baseline
●Balance drift:< 5 μg / h
●Zui sample weighing:35000 mg(including crucible), corresponding toTGAmeasuring range
●Sample volume: the largest5 cm3(For)TGACrucible)
●Enthalpy accuracy:1% (In)
●Analysis of escaping gases:QMS, GC-MSWith/orFT-IRCombined use
3、 Software functions:
STA 449 F5 Jupiter ® -software function
STA 449 F5 Jupiter ®The measurement and analysis software is based onWindows ®The system'sProteus ®Software package. The software itself is self-contained and does not require complex custom configuration. The software has a very user-friendly interface, automated programs, and context sensitive help systems that can help you reduce workload and save time.Proteus ®Associated with each specific instrument and can also be installed on other computers.
Conventional software features
●Multi tasking: capable of simultaneously performing measurement and data analysis
●Multi module: using the same computer to operate different instruments
●Comprehensive analysis: Comparing and analyzing within the same graphSTA,DSC,TGA,DIL,TMAWithDMAmeasure
●Adjustable coordinate range
●Visualization and Data Export
●Calculate first-order and second-order differentials, including peak temperature
●Storage and Recovery Analysis Status
●Context related help system
●The software is developed throughISOCertified professional subsidiary development and design
DSCRelated characteristics
●Measure the starting point, peak temperature, inflection point, and termination temperature, and perform automatic peak search
●Analyze the peak area (enthalpy) of heat release and absorption, and provide multiple baseline types to choose from; Support partial peak area analysis
●Comprehensive analysis: Comparing and analyzing within the same graph/Or analyzeSTA,DSC,TGA,DIL,TMA、DMAWaiting for various measurement curves
●Comprehensive analysis of glass transition temperature
●crystallinity
●OIT(Oxidation induction time)
●Specific heat measurement (optional)
TGARelated characteristics
●Quality change, unit%ormg
●Automatic analysis of quality change steps, including residual quality analysis
●Starting and ending points of extrapolation
●Automatic baseline correction function(TGA-BeFlat ®), used for automatic correction of measurement influencing factors
●c-DTA ®: Computational typeDTASignal, analyze characteristic temperature and peak area (single)TGAOptional measurement functions
●Super-Res ®: Rate control quality change (optional)
Related advanced software:
●Peak Separation Software
●Dynamics software
4、 Related attachments
STA 449 F5 Jupiter ® -Related attachments
Two methods, a more effective combination
The system is equipped with user replaceableTGA-DSCSensors that can performDSC, or synchronizedTGA-DSCMeasurement can also be usedASCPerform automatic sampling. Additionally, it also providesTGAandTG-DTASensors.
atmosphere-useMFCandAutoVacPerform * control
Three built-in mass flow controllers can optimize the control of the blowing gas and protective atmosphere around the sample. The use of vacuum pumping and inert atmosphere replacement can further control the atmosphere around the sample, and can also be applied to powder samples and other samples that are difficult to vacuum. This automatic vacuum(AutoVac)The device simplifies the operation of the vacuum process. The device includes a vane rotary pump system that can be fully operated through software.
Various crucibles-Suitable for your requirements
We offer crucibles of various materials and sizes. The most common crucible materials include alumina and platinum. There are also crucibles made of other materials, such as gold, zirconia, etc. The crucible can be equipped with a perforated or unperforated crucible cover. With such a wide range of choices, there is always one that meets your testing requirements.
Automatic sampler-A worry free choice
Automatic sampler provides up to 20 A sample grade that can be used forTGAorTGA-DSCMeasurement. The automatic sampler ensures the optimal injection position and maximum processing capacity of the sample. By pre writing the injection sequence, it is possible to fully utilize the evening or weekend time, and the instrument will measure according to the pre programmed schedule.
Efficient and reliable-A choice you won't regret
Everything is ready-Used in conjunction with gas analysis instruments for escaping gases
STA 449 F5(including versions equipped with automatic samplers) can be used withQMS、FTIRorGC-MSUsed in conjunction to analyze the composition of escaping gases. The instrument can also be connected simultaneouslyQMSWithFTIR, orGC-MSWithFTIR.