The main detection methods for melamine include liquid chromatography, gas chromatography-mass spectrometry, liquid chromatography-mass spectrometry, etc. Among them, liquid chromatography has the advantages of high sensitivity, accuracy, reliability, and low instrument cost, making it an ideal method for detecting melamine.
The main detection methods for melamine include liquid chromatography, gas chromatography-mass spectrometry, liquid chromatography-mass spectrometry, etc. Among them, liquid chromatography has the advantages of high sensitivity, accuracy, reliability, and low instrument cost, making it an ideal method for detecting melamine.
Dalian Yilite Analytical Instrument Co., Ltd. has conducted extensive experiments and provided you with a complete solution that complies with the national standard for testing melamine, including analytical methods and recommended instrument configurations.
Recommended configuration for San melamine detection liquid chromatography instrument
Serial Number
name
quantity
Equivalent efficiencyLiquid chromatography system
1
P3100 high-pressure constant current pump
1 unit
2
UV3100 UV Visible Detector
1 unit
3
Rheodyne 7725i high-pressure six way injection valve
1 piece
4
ZJ-1 valve bracket
1 piece
5
TD-1-15 gradient mixer (optional)
1 piece
6
W5100 Chromatographic Data Workstation
1 set
7
O3100 chromatographic column constant temperature box
1 unit
8
TP3100 solvent tray
1 unit
chromatographic column
9
Elite MSP C18san melamine specific column
1 unit
configuration(More features, user-friendly configuration, higher work efficiency)
10
DG3100 online deaerator
1 unit
11
S3100 automatic sampler
1 unit
San analysis method package for testing melamine
Serial number
name
Specification and model
1
citric acid
analytical pure
2
sodium octane sulfonate
HPLC
3
San melamine standard
CAS108-78-01, Purity ≥ 99.0%
4
Water based filter membrane (100 pieces/box)
φ50mm,0.45μm
5
Organic filter membrane (100 pieces/box)
φ50mm,0.45μm
6
Needle type organic phase filter (100 pieces/pack)
φ13mm,0.22μm
7
Mixed cation solid-phase extraction column (50 tubes/box)
HyperSep Retain-CX,60mg/3mL
Pre treatment configuration package for melamine testing
Serial Number
name
Specification and model
1
Ultrasonic water bath
AS3120 type, 3L, power: 120W
2
Diaphragm Vacuum Pump
Gm type
3
Solvent filter
1000mL
4
analytical balance
AL104, Sensitivity 0.0001g
JD60-4,0.0001g
5
pH meter
FE20K acidity meter
6010 acidity meter
6
centrifuge
TG16G, 16000 RPM, 6 × 50mL
TD5G, 5000 RPM, 12 × 10mL
7
SPE
SPE-12
8
nitrogen concentration
PGC-01D
9
Vortexers
QL-861
10
mortar
90, alumina
performance index
Analysis speed
Analysis time<25 minutes
linear range
≥80µg/mL
detection limit
0.016mg/kg